Fulvestrant intermediate A
9-Bromo-1-nonanol
CAS: 55362-80-6
Molecular Formula: C9H19BrO
Fulvestrant intermediate A - Names and Identifiers
| Name | 9-Bromo-1-nonanol |
| Synonyms | Br-9C-OH 9-bromononan-1-ol 9-Bromo-1-nonanol 9-bromo nonan-1-ol 1-Nonanol, 9-bromo- 1-Hydroxy-9-broMononane Fulvestrant intermediate A |
| CAS | 55362-80-6 |
| EINECS | 611-262-6 |
| InChI | InChI=1/C9H19BrO/c10-8-6-4-2-1-3-5-7-9-11/h11H,1-9H2 |
| InChIKey | USJDOLXCPFASNV-UHFFFAOYSA-N |
Fulvestrant intermediate A - Physico-chemical Properties
| Molecular Formula | C9H19BrO |
| Molar Mass | 223.15 |
| Density | 1.2107 (rough estimate) |
| Melting Point | 33-35 °C (lit.) |
| Boling Point | 125-126 °C/2 mmHg (lit.) |
| Flash Point | >230°F |
| Solubility | Soluble in dichloromethane, ethyl acetate and hexane. |
| Vapor Presure | 0.000545mmHg at 25°C |
| Appearance | Bright yellow powder |
| BRN | 1737525 |
| pKa | 15.19±0.10(Predicted) |
| Storage Condition | Keep in dark place,Sealed in dry,Room Temperature |
| Stability | Stable. Incompatible with strong oxidizing agents. |
| Sensitive | Sensitive to heat and air |
| Refractive Index | 1.5700 (estimate) |
| MDL | MFCD00063348 |
Fulvestrant intermediate A - Risk and Safety
| Hazard Symbols | Xi - Irritant |
| Risk Codes | 36/37/38 - Irritating to eyes, respiratory system and skin. |
| Safety Description | S26 - In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. S36 - Wear suitable protective clothing. |
| WGK Germany | 3 |
| TSCA | Yes |
| HS Code | 29055900 |
Fulvestrant intermediate A - Reference Information
| use | 9-bromo-1-nonanol is an organic intermediate, which can be obtained by bromination from 1,9-nonanediol as raw material. There are reports that it can be used to prepare sex pheromone of Spodoptera litura. |
| preparation | 40g of 1,9-nonanediol, 550ml of toluene and 35ml of 48% HBr aqueous solution were added into the container for stirring reflux reaction for 12h, 8ml of 48% HBr aqueous solution was added for reflux reaction for 15h, cooled to room temperature and diluted with n-hexane, wash with saturated NaHCO3 solution and salt water, dry with anhydrous Na2SO4, and distill under reduced pressure to obtain colorless transparent liquid 9-bromo-1 nonanol. |
| NIST chemical information | The information is: webbook.nist.gov provides (external link) |
| EPA chemical information | The information is: offered by ofmpub.epa.gov (external link) |
Last Update：2024-04-10 22:29:15
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